HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 21442879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-(8-Hydroxy-7-nitroquinolin-5-yl)ethan-1-one | HCID 21442886 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21442879 | HCID 21442879 | — |
Reaction Steps
10.5 g of triethylamine are added to a solution of 23 g of 5-acetyl-7-nitro-8-hydroxyquinoline in 150 ml of tetrahydrofurane and 9.5 g of chloroformic acid methyl ester are slowly added dropwise to this mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04017627 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-601db3236799463c9bad2d54e2d3f9e7 |
| Source note | uspto-grants-1977_04 |