Acetyl chloride → HCID 21442817, compound

Participants

Reaction Steps

To a solution of 5-(2-morpholinylmethyl)-10,11-dihydro-5H-dibenz[b,f]azepine (0.34 g) in anhydrous benzene was added excess acetyl chloride under ice cooling. After stirring for 4 hours, the reaction mixture was washed with aqueous 2N sodium hydroxide and then with water, dried and evaporated to afford 5-(4-acetyl-2-morpholinylmethyl)-10,11-dihydro-5H-dibenz[b,f]azepine as an oily substance.

Provenance & Evidence