HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 178423600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 178423599 | HCID 178423599 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178423600 | HCID 178423600 | 43% |
Reaction Steps
A solution of 3-hydroxy-5-methyl-1,4-naphthoquinone (1.9g) in chloroform (200ml) was nitrated with fuming nitric acid according to example 1(a). A yield of 1.01g (43%) of material of m.p. 148°-149° C (d) was obtained. (Found; C, 56.69; H, 3.16; N, 5,73; C11H7NO5 requires; C, 56.66; H, 3.03; N, 6.01%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04017639 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-a564b2b35f114dd18ff50e133f27c249 |
| Source note | uspto-grants-1977_04 |