HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Amino-3,3-diphenylpropanoic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenylalanine,N-acetyl--phenyl- | HCID 11022400 | — |
| Product | 2-Amino-3,3-diphenylpropanoic acid hydrochloride | HCID 19772460 | — |
Reaction Steps
A solution (21 mL) of 2-acetylamino-3,3-diphenylpropanoic acid (2.83 g, 10 mmol) in concentrated hydrochloric acid was stirred at 90° C. for 5 hrs, and the reaction mixture was cooled in an ice bath to allow solid precipitation. The solid was collected by filtration and dried to give the title compound (2.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427688B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-180659972f66413a9d3b5f339b90f27f |
| Source note | uspto-grants-2008_09 |