HRID32864

反应详情

EQUATION

反应方程式

HRID 32864 的结构方程式

PROCEDURE

实验过程

A solution (21 mL) of 2-acetylamino-3,3-diphenylpropanoic acid (2.83 g, 10 mmol) in concentrated hydrochloric acid was stirred at 90° C. for 5 hrs, and the reaction mixture was cooled in an ice bath to allow solid precipitation. The solid was collected by filtration and dried to give the title compound (2.65 g).

WORKUP

后处理

  1. temperaturethe reaction mixture was cooled in an ice bath
  2. customsolid precipitation
  3. filtrationThe solid was collected by filtration
  4. customdried