Hydrochloric Acid → HCID 3303868, compound
Reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([CH:6]=[N:7][OH:8])=[CH:4][CH:3]=1.[ClH:11]>>[Cl:11][C:6](=[N:7][OH:8])[C:5]1[CH:9]=[CH:10][C:2]([CH3:1])=[CH:3][CH:4]=1Participants
3
Procedure
27 g (0.2 mol) of 4-methylbenzaldoxime was chlorinated in the same manner as described in Example 9 (A) in 150 ml of 8N hydrochloric acid to give 28 g of the product as white crystals having a melting point of 60°-70° C. Yield, about 82%.
Sources & evidence
- ORD record
- ord-fb038ced68f448d58ad4d63edc777740
- Source dataset
- uspto-grants-1977_04
- Patent number
- US04018645
Reaction notes
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