HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 4-Methoxy[1]benzothieno[3,2-d][1,2,3]triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 12269873 | HCID 12269873 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Methoxy[1]benzothieno[3,2-d][1,2,3]triazine | HCID 323430 | — |
Reaction Steps
A 2.2 g. portion of the product of Example 1 was stirred at reflux temperature in 100 ml. of methanol with 0.7 g. of sodium methoxide for one hour. When the reaction mixture was cooled, the product, 1.9 g. of 4-methoxy[1]-benzothieno[3,2-d]-v-triazine, m.p. 165°-167° C., crystallized and needed no further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018768 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-41716bf0ef4347d887d34487b671ca35 |
| Source note | uspto-grants-1977_04 |