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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 328674Generated: October 29, 2026

Sodium Methoxide → 4-Methoxy[1]benzothieno[3,2-d][1,2,3]triazine

https://huagongshe.com/reaction/328674

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 12269873HCID 12269873—
SolventMethanolHCID 887—
Product4-Methoxy[1]benzothieno[3,2-d][1,2,3]triazineHCID 323430—

Reaction Steps

A 2.2 g. portion of the product of Example 1 was stirred at reflux temperature in 100 ml. of methanol with 0.7 g. of sodium methoxide for one hour. When the reaction mixture was cooled, the product, 1.9 g. of 4-methoxy[1]-benzothieno[3,2-d]-v-triazine, m.p. 165°-167° C., crystallized and needed no further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04018768
Source datasetuspto-grants-1977_04
ORD IDord-41716bf0ef4347d887d34487b671ca35
Source noteuspto-grants-1977_04