HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (2R,3R)-3-Amino-5,8-dimethoxy-1,2,3,4-tetrahydronaphthalen-2-ol | HCID 13146838 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 131710713 | HCID 131710713 | — |
Reaction Steps
A solution of 3.7 g of trans-3-amino-1,2,3,4-tetrahydro-5,8-dimethoxy-2-naphthalenol is isopropanol is converted to the hydrochloride salt by adding a solution of hydrogen chloride in isopropanol. The salt is precipitated by adding ether and recrystallized twice from isopropanol to give 1.3 g of the title compound, melting point 213°-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018773 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-a2d95f76af974fd995879fcfe101f8b5 |
| Source note | uspto-grants-1977_04 |