HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 3,4-dinitrobenzoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 3,4-Dinitrobenzoic acid | HCID 10709 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3,4-dinitrobenzoyl Chloride | HCID 11806491 | — |
Reaction Steps
Fifty-three grams (0.25 mole) of 3,4-dinitrobenzoic acid, 500 ml. of benzene, 65 g. (0.51 mole) of oxalyl chloride and 1 ml. of pyridine were reacted according to Example 2 (A), first paragraph, to provide 3,4-dinitrobenzoyl chloride as a crude oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018790 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-839dba5eea18470c8312ecc4e251e62e |
| Source note | uspto-grants-1977_04 |