HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → (3-trifluoromethyl-phenoxy)-acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1-(2,2-Diethoxyethoxy)-3-(trifluoromethyl)benzene | HCID 12661800 | — |
| Solvent | Water | HCID 962 | — |
| Product | (3-trifluoromethyl-phenoxy)-acetaldehyde | HCID 11252687 | — |
Reaction Steps
A mixture of 3-trifluoromethylphenoxyacetaldehyde diethyl acetal (146.3 g.; 0.527 mole), acetone (600 ml.), water (550 ml.), and concentrated sulfuric acid (3.5 ml.) is heated under reflux for 22 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018802 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-cb144d0b78e946e5b21ad719980ac65f |
| Source note | uspto-grants-1977_04 |