HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21440148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | HCID 21440132 | HCID 21440132 | — |
| Reactant | HCID 21440165 | HCID 21440165 | — |
| Product | HCID 21440148 | HCID 21440148 | — |
Reaction Steps
By replacing in Example 6, step B, ethyl 4-benzoyl3-hydroxy-5-nitrobenzoate and ethyl iodide with equimolar amounts of ethyl 3-hydroxy-4-(4'-methylbenzoyl)-5-nitrobenzoate and n-butyl iodide respectively and following the procedure described, 3-n-butoxy-4-(4'-methylbenzoyl)5-nitrobenzoic acid crystallizing with 0.5mole of ethanol is obtained with a melting point of 162.5°-163° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018794 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-1571820823a243b9b2ad7b53c1059800 |
| Source note | uspto-grants-1977_04 |