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HRID328948

反应详情

EQUATION

反应方程式

HRID 328948 的结构方程式

REACTANTS

反应物

5
结构：CCO
HCID702

Ethanol

C2H6O

结构：CCI
HCID6340

Ethane, iodo-

C2H5I

结构：CCCCI
HCID10962

1-Iodobutane

C4H9I

结构：CCOC(=O)c1cc(O)c(C(=O)c2ccccc2)c([N+](=O)[O-])c1
HCID21440132

未命名化合物

结构：CCOC(=O)c1cc(O)c(C(=O)c2ccc(C)cc2)c([N+](=O)[O-])c1
HCID21440165

未命名化合物

PRODUCTS

生成物

1
结构：CCCCOc1cc(C(=O)O)cc([N+](=O)[O-])c1C(=O)c1ccc(C)cc1
HCID21440148

未命名化合物

PROCEDURE

实验过程

By replacing in Example 6, step B, ethyl 4-benzoyl3-hydroxy-5-nitrobenzoate and ethyl iodide with equimolar amounts of ethyl 3-hydroxy-4-(4'-methylbenzoyl)-5-nitrobenzoate and n-butyl iodide respectively and following the procedure described, 3-n-butoxy-4-(4'-methylbenzoyl)5-nitrobenzoic acid crystallizing with 0.5mole of ethanol is obtained with a melting point of 162.5°-163° C.