HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 88821752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12222283 | HCID 12222283 | — |
| Product | HCID 88821752 | HCID 88821752 | — |
Reaction Steps
19.4 g of 3-amidinophenoxyacetic acid were heated under reflux, while well stirring, for 2 hours with 70 ml of thionyl chloride. After cooling, filtration with suction and washing with anhydrous diethyl ether, 21 g of 3-amidinophenoxyacetic acid chloride hydrochloride were obtained; decomposition point 149° to 151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018933 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-16d9569b6f38433aa82e185d50c4b9db |
| Source note | uspto-grants-1977_04 |