HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21438917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20352711 | HCID 20352711 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21438917 | HCID 21438917 | — |
Reaction Steps
A suspension of the sodium salt of (2,4-dimethyl-5-pyrimidylcarbonyl)-acetone in anhydrous toluene is saturated with hydrogen chloride and then reacted with thionyl chloride in a known manner. Reduction of the reaction product gives 1-(2,4-dimethyl-5-pyrimidyl)-3-chloro-butan-1-ol hydrochloride which is used without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04020071 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-3010d82df18a409a9253a931bf65bb1a |
| Source note | uspto-grants-1977_04 |