2-Fluorophenol → HCID 22759250, compound

HRID 329290Notes

Reaction equation

[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].[C:9]([CH:12]([CH2:22][CH2:23][CH2:24][CH:25]([OH:38])[CH2:26]OC1C=CC(C(C)(C)C)=CC=1)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19]([OH:21])=[O:20])(=[O:11])[CH3:10]>>[C:9]([CH:12]([CH2:22][CH2:23][CH2:24][CH:25]([OH:38])[CH2:26][O:8][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[F:1])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19]([OH:21])=[O:20])(=[O:11])[CH3:10]

Participants

Reactant 2

HCID 97072-Fluorophenol

HCID 22759343HCID 22759343, compound

Product 1

HCID 22759250HCID 22759250, compound

Procedure

The synthesis of this compound is carried out by the procedure of Example 10 except that an equivalent amount of 2-fluorophenol is substituted for the 4-tertbutylphenol of Example 10. The title compound is obtained as a viscous oil after purification by silica gel column chromatography.

Workup

customThe synthesis of this compound

Sources & evidence

ORD record: ord-91fb60493b294738aeff98c36638a26a
Source dataset: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04020177

Reaction notes

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