HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 21439156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 5H-Dibenzo(a,d)cycloheptene-2-acetic acid, alpha-methyl-5-oxo- | HCID 173910 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21439156 | HCID 21439156 | — |
Reaction Steps
0.45 G. of 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionic acid was dissolved in ethyl acetate and isopropylamine is added dropwise until no more precipitate is formed. The precipitate is filtered off and recrystallized from acetone to afford isopropylammonium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate (m.p. 176°-180° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04020094 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-700b1925030f4f79a7de0179f80e94f3 |
| Source note | uspto-grants-1977_04 |