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HRID329334

反应详情

EQUATION

反应方程式

HRID 329334 的结构方程式

REACTANTS

反应物

2
反应SMILES：CC(C)N
HCID6363

Isopropylamine

C3H9N

反应SMILES：CC(C(=O)O)c1ccc2c(=O)c3ccccc3ccc2c1
HCID173910

2-(5-Oxo-5H-dibenzo[a,d][7]annulen-2-yl)propanoic acid

C18H14O3

PRODUCTS

产物

1
反应SMILES：CC(C(=O)[O-])c1ccc2c(=O)c3ccccc3ccc2c1.CC(C)[NH3+]
HCID21439156

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

0.45 G. of 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionic acid was dissolved in ethyl acetate and isopropylamine is added dropwise until no more precipitate is formed. The precipitate is filtered off and recrystallized from acetone to afford isopropylammonium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate (m.p. 176°-180° C).

WORKUP

后处理

  1. customis formed
  2. filtrationThe precipitate is filtered off
  3. customrecrystallized from acetone