HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenethyl bromide → 7-Nitro-3-(4-nitrophenethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine hemihydrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenethyl bromide | HCID 79266 | — |
| Reactant | 7-Nitro-2,3,4,5-tetrahydro-1H-benzo[D]azepine | HCID 11310042 | — |
| Product | 7-Nitro-3-(4-nitrophenethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine hemihydrate | HCID 88599941 | — |
Reaction Steps
The title compound was prepared similarly to Preparation 2 by the reaction of 7-nitro-1,2,4,5-tetrahydro-3H-3-benzazepine (0.5 g) and 4-nitrophenethyl bromide (0.6 g), which, after 18 hours reflux, gave the title compound as an oil, yield 0.29 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04891372 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-2b708feff62a4e0a8d1dae268f1ea493 |
| Source note | uspto-grants-1990_01 |