HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19872053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19872055 | HCID 19872055 | — |
| Product | HCID 19872053 | HCID 19872053 | — |
Reaction Steps
3-[2-(4-Acetylamino-3-methylphenoxy)ethyl]-7-nitro-1,2,4,5-tetrahydro-3H-3-benzazepine (1 g) was stirred in 6M hydrochloric acid (20 ml) at 90° for 18 hours. After cooling, the precipitate was collected by filtration and recrystallised from ethanol to give the title compound, yield 0.65 g, m.p. 253°-256°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04891372 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-074708e098b142c7a90544498a37bac1 |
| Source note | uspto-grants-1990_01 |