HCID 13986694, compound → HCID 13986697, compound

HRID 329438Notes

Reaction equation

HRID 329438 reaction equation
CC1C=CC=C(C)C=1NCCCCC1C=NC=CC=1.[CH3:20][C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([CH3:27])[C:22]=1[NH:28][C:29](=O)[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][C:35]1[CH:36]=[N:37][CH:38]=[CH:39][CH:40]=1>>[CH3:27][C:23]1[CH:24]=[CH:25][CH:26]=[C:21]([CH3:20])[C:22]=1[NH:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][C:35]1[CH:36]=[N:37][CH:38]=[CH:39][CH:40]=1

Participants

3

Reactant 2

HCID 13986694HCID 13986694, compoundHCID 13986696HCID 13986696, compound

Product 1

HCID 13986697HCID 13986697, compound

Procedure

N-(2,6-Dimethylphenyl)-3-pyridinehexanamine was prepared in a manner similar to that employed above for preparing N-(2,6-dimethylphenyl)-3-pyridinebutanamine. Starting with 6.4 g of N-(2,6-dimethylphenyl)-3-pyridinehexanamide, there was obtained 3.6 g of a yellow oil which was purified by silica gel chromatography eluting with 1:1 ethyl acetate-hexane to give 2.8 g of N-(2,6-dimethylphenyl) -3-pyridinehexanamine as an oil, bp 215°-230° C./0.1 mm.

Sources & evidence

ORD record
ord-877d5413be6f41859fe452856d6174c8
Source dataset
uspto-grants-1990_01
Patent number
US04891429

Reaction notes

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