HCID 13986694, compound → HCID 13986697, compound

Participants

Reaction Steps

N-(2,6-Dimethylphenyl)-3-pyridinehexanamine was prepared in a manner similar to that employed above for preparing N-(2,6-dimethylphenyl)-3-pyridinebutanamine. Starting with 6.4 g of N-(2,6-dimethylphenyl)-3-pyridinehexanamide, there was obtained 3.6 g of a yellow oil which was purified by silica gel chromatography eluting with 1:1 ethyl acetate-hexane to give 2.8 g of N-(2,6-dimethylphenyl) -3-pyridinehexanamine as an oil, bp 215°-230° C./0.1 mm.

Provenance & Evidence