HCID 67870777, compound → HCID 67870769, compound

Participants

Reaction Steps

Following a procedure similar to that described in Preparation 4, but using a solution of 1.300 g of dl-cis-2-benzyloxymethyltetrahydropyran-3-yl N-heptadecylcarbamate (prepared as described in Preparation 65) in 30 ml of ethanol and 0.819 g of 10% w/w palladium on activated carbon, 0.977 g of the title compound was obtained as crystals. These crystals melted at 81.0°-82.0° C. after recrystallisation from diethyl ether.

Provenance & Evidence