Sodium Acetate → HCID 15052053, compound

Participants

Reaction Steps

This compound was prepared in a manner analogous to that of Example 10, using 2.0 grams (0.004 mole) of 2-[[2-bromo-4-[(2-carboxyphenyl)carbonylamino]phenyl]-methyl]-4,4-dimethyl-3-isoxazolidinone and 5.0 grams (0.061 mole) of sodium acetate in 50 mL of acetic anhydride. The solid was recrystallized from ethyl acetatehexane to yield 2-[(2-bromo-4-phthalimidophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone; m.p. 158°-159° C.

Provenance & Evidence