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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 329572Generated: November 1, 2026

N-Methylhydrazinecarbothioamide → HCID 14348270, compound

https://huagongshe.com/reaction/329572

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-MethylhydrazinecarbothioamideHCID 2723853—
ReactantHCID 2755381HCID 2755381—
SolventEthanolHCID 702—
ProductHCID 14348270HCID 14348270—

Reaction Steps

45.11 g (0.127 mol) Methyl 3,3-dibenzylthio-2-cyanoacrylate and 13.35 g (0.127 mol) 4-methylthiosemicarbazide in 225 ml ethanol were heated under reflux for 10 hours. After cooling, the product was suction filtered, washed with ether and dried.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04892576
Source datasetuspto-grants-1990_01
ORD IDord-fcc319077ae3449b8a1b80c24d5f9896
Source noteuspto-grants-1990_01