反应详情

4,01 g (29.9 mmol) of 2,2-difluoro-4-pentenoate acid are dissolved in 20 ml of methanol, and 1 equivalent of NaOCH3 in methanol is added at room temperature (RT). After evaporation in the RE, 4.65 g (100%) of colourless crystals of melting point 168°-170° C. (decomposition) remain.

1. customAfter evaporation in the RE, 4.65 g (100%) of colourless crystals of melting point 168°-170° C. (decomposition)