HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 28306209, compound → HCID 23686291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 28306209 | HCID 28306209 | — |
| Reactant | HCID 178418582 | HCID 178418582 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23686291 | HCID 23686291 | — |
Reaction Steps
4,01 g (29.9 mmol) of 2,2-difluoro-4-pentenoate acid are dissolved in 20 ml of methanol, and 1 equivalent of NaOCH3 in methanol is added at room temperature (RT). After evaporation in the RE, 4.65 g (100%) of colourless crystals of melting point 168°-170° C. (decomposition) remain.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04892962 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-d3f794bb5082473c9d03269c5776d798 |
| Source note | uspto-grants-1990_01 |