HRID330055

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)C[C@H](NC(=O)OC(C)(C)C)C(=O)N[C@@H](CCCCNC(=O)OCc1ccccc1)C(=O)O

HCID13857776

未命名化合物

PRODUCTS

生成物

结构：CC(C)C[C@H](N)C(=O)N[C@@H](CCCCNC(=O)OCc1ccccc1)C(=O)O

HCID121596127

未命名化合物

收率 140.7%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID22641269

未命名化合物

PROCEDURE

实验过程

In 90.8 ml of 2N HCl/AcOH, 22.8 g (36.3 mmol) of BOC-Leu-Lys(Z)-CHA was dissolved and reacted at room temperature for 2 hours. After the reaction, deposited crystals were reprecipitated in 1000 ml of ether, filtered and dried to yield 20.1 g (98.0%) of H-Leu-Lys(Z)-CHA.HCl.

WORKUP

后处理

customreacted at room temperature for 2 hours
customAfter the reaction
customwere reprecipitated in 1000 ml of ether
filtrationfiltered
customdried