HuagongsheHuagongshe Chemistry Print Report · For research reference only
BOC-Leu-Lys(Z) → H-Leu-Lys(Z)-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | BOC-Leu-Lys(Z) | HCID 13857776 | — |
| Solvent | Acetate-hydrochloric acid | HCID 22641269 | — |
| Product | H-Leu-Lys(Z)-OH | HCID 121596127 | 140.7% |
Reaction Steps
In 90.8 ml of 2N HCl/AcOH, 22.8 g (36.3 mmol) of BOC-Leu-Lys(Z)-CHA was dissolved and reacted at room temperature for 2 hours. After the reaction, deposited crystals were reprecipitated in 1000 ml of ether, filtered and dried to yield 20.1 g (98.0%) of H-Leu-Lys(Z)-CHA.HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04894438 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-1accbc79cf234868ae7a2cf2f1966d85 |
| Source note | uspto-grants-1990_01 |