Dichloromethane → HCID 178419234, compound

HRID 330223Notes

Reaction equation

HRID 330223 reaction equation
C(Cl)Cl.[O:4]=[CH:5][C@@H:6]([C@H:8]([C@@H:10]([C@@H:12]([CH2:14][OH:15])[OH:13])[OH:11])[OH:9])[OH:7].O=[CH:17][C@@H:18]([C@H:20]([C@@H:22]([C@@H:24]([CH2:26]O)O)O)O)[OH:19].C(O[BH:33][O:34][CH2:35][CH2:36][CH2:37][CH3:38])CCC>O>[O:4]=[CH:5][C@@H:6]([C@H:8]([C@@H:10]([C@@H:12]([CH2:14][OH:15])[OH:13])[OH:11])[OH:9])[OH:7].[C:35]1([O:34][BH:33][O:19][C:18]2[CH:17]=[CH:26][CH:24]=[CH:22][CH:20]=2)[CH:36]=[CH:37][CH:38]=[CH:6][CH:5]=1

Participants

5

Reactant 3

HCID 6344DichloromethaneHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanalHCID 178450001HCID 178450001, compound

Product 1

HCID 178419234HCID 178419234, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of 100 mg/dL of glucose bis phenylboronate and dry methylene chloride was prepared and applied to CLINISTIX® glucose test strip pad. No color development was observed. The pads were then wetted with water and in 2 or 3 minutes color development was observed. Glucose bis butylboronate was similarly applied to CLINISTIX® strips. Again no color was observed upon application. After wetting with water strong color development was observed in 10 to 15 seconds.

Sources & evidence

ORD record
ord-898a566d03a44b9686d699cb891d1279
Source dataset
uspto-grants-1990_01
Patent number
US04895798

Reaction notes

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