HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 85556120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 131716254 | HCID 131716254 | — |
| Product | HCID 85556120 | HCID 85556120 | — |
Reaction Steps
BOC-NHCH2CH(OH)CH2SO2CH(CH3)2 (3.19 g, 11.35 mmole) was dissolved in 75 ml CH2Cl2 and purged with HCl gas over two hours. The mixture was stripped, triturated with ethyl ether, and filtered. The solid was washed with ethyl ether and dried giving 2.21 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04895834 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-20a2dd9e5e2640a29f7ddf190335c505 |
| Source note | uspto-grants-1990_01 |