HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 11287703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 11817172 | HCID 11817172 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 11287703 | HCID 11287703 | 79% |
Reaction Steps
5.0 g (0.0225 mole) of the product of Step A and 10 g (0.115 mole) of manganese dioxide were stirred under reflux in 500 ml of chloroform for 2 hours. The mixture was filtered hot through celite and evaporated under reduced pressure to obtain 3.92 g (79% yield) of 7-methoxy-imidazo[2,1-b]benzothiazole-2-carboxaldehyde as colorless crystals melting at 214° to 215° C. (EtOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04895863 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-6105d653a57a475c938ccfa0b4b62d87 |
| Source note | uspto-grants-1990_01 |