Valproic Acid → HCID 86743698, compound

HRID 330309Notes

Reaction equation

HRID 330309 reaction equation
[OH-].[Ca+2:2].[OH-].[C:4]([OH:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8]>CC(C)=O>[C:4]([O-:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8].[C:4]([OH:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8].[C:4]([OH:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8].[C:4]([OH:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8].[C:4]([O-:13])(=[O:12])[CH:5]([CH2:9][CH2:10][CH3:11])[CH2:6][CH2:7][CH3:8].[Ca+2:2]

Participants

4

Reactant 2

HCID 3121Valproic AcidHCID 6093208Calcium Hydroxide

Product 1

HCID 86743698HCID 86743698, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

29.6 g of pulverized calcium hydroxide were stirred in a solution of 288.4 g of valproic acid in 1300 ml of acetone and the mixture was refluxed for 2 hours.

Workup

  1. temperaturethe mixture was refluxed for 2 hours

Sources & evidence

ORD record
ord-28686e7d891744ba83df6af08194ca7b
Source dataset
uspto-grants-1990_01
Patent number
US04895873

Reaction notes

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