HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → Benzoic acid, 2-[4-(1,1-dimethylpropyl)benzoyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | tert-Amylbenzene | HCID 16295 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 178418750 | HCID 178418750 | — |
| Product | Benzoic acid, 2-[4-(1,1-dimethylpropyl)benzoyl]- | HCID 116561 | 80% |
Reaction Steps
74 g (0.5 mole) of phthalic anhydride were reacted with 128 g (1.05 moles) of AlCl3 and 25 g (0.2 mole) of diethylzinc in 74 g of tert-amylbenzene, similarly to Example 1. After the mixture had been worked up, 118 g (80% of theory) of pure 2-(4'-tert-amylbenzoyl)-benzoic acid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04895984 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-b98a8a59792a4626bfb371f71908a457 |
| Source note | uspto-grants-1990_01 |