HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13974075, compound → HCID 13974076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13974075 | HCID 13974075 | — |
| Solvent | Ethanol hydrochloride | HCID 21887872 | — |
| Product | HCID 13974076 | HCID 13974076 | 75% |
Reaction Steps
9.66 g (15 mmol) of (8) were treated for 6 hours with 30 ml of 2N HCl/EtOH solution (5:5). After extraction with EtOAc, 7.2 g of crude sample were obtained. After silica gel column separation, using EtOAc/Hexane (6:4) as solvent, 6.3 g of (9) (75% yield) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04897412 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-2cadf2d5c4a2484fa8023b4a5bb5d5eb |
| Source note | uspto-grants-1990_01 |