Hydrochloric Acid → HCID 14457258, compound

HRID 330535Notes

Reaction equation

HRID 330535 reaction equation
[F:1][C:2]1([F:16])[O:6][C:5]2[CH:7]=[CH:8][C:9]([N:11]=[C:12]3[S:15][CH2:14][S:13]3)=[CH:10][C:4]=2[O:3]1.[ClH:17]>C(OCC)C>[ClH:17].[F:16][C:2]1([F:1])[O:6][C:5]2[CH:7]=[CH:8][C:9]([N:11]=[C:12]3[S:13][CH2:14][S:15]3)=[CH:10][C:4]=2[O:3]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 14457257HCID 14457257, compound

Product 1

HCID 14457258HCID 14457258, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

10.0 g (0.0357 mol) N-(2,2-Difluoro-1,3-benzodioxol-5-yl)-1,3-dithietan-2-imine was dissolved in 300 ml diethyl ether and, under vigorous stirring and ice cooling, hydrogen chloride gas was passed in. The precipitated crystals were separated and dried.

Workup

  1. customThe precipitated crystals were separated
  2. customdried

Sources & evidence

ORD record
ord-4de3aaea58cd4841a90a7d95cadd6e58
Source dataset
uspto-grants-1990_01
Patent number
US04897415

Reaction notes

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