HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3,3-bis(4-fluorophenyl)-2-[2-(1-methylethyl) 2H-tetrazol-5-yl]-2-propenoate → 3,3-Bis(4-fluorophenyl)-2-[2-(1-methylethyl)-2H-tetrazol-5-yl]-2-propenal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3,3-bis(4-fluorophenyl)-2-[2-(1-methylethyl) 2H-tetrazol-5-yl]-2-propenoate | HCID 14723868 | — |
| Reactant | ethyl 3,3-bis(4-fluorophenyl)-2-[1-(1-methylethyl)-1H-tetrazol-5-yl]-2-propenoate | HCID 14723869 | — |
| Product | 3,3-Bis(4-fluorophenyl)-2-[2-(1-methylethyl)-2H-tetrazol-5-yl]-2-propenal | HCID 14723874 | 88% |
Reaction Steps
The general procedure of Example 21, Steps A, B, C, and D were repeated, except that the ethyl 3,3-bis(4-flurophenyl)-2-[1-(1-methylethyl)-1H-tetrazol-5-yl]-2-propenoate utilized therein was replaced by ethyl 3,3-bis(4-fluorophenyl)-2-[2-(1-methylethyl)-2H-tetrazol-5-yl]-2-propenoate and there was thereby produced in 88% yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04897490 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-c524880d3d194212948d1c2723140bcf |
| Source note | uspto-grants-1990_01 |