1,3-Dibromobenzene → HCID 66962129, compound

HRID 331037Notes

Reaction equation

Br[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Br:8])[CH:3]=1.[CH3:9][NH:10][CH:11]1[CH2:15][CH2:14][CH2:13][CH2:12]1>>[Br:8][C:4]1[CH:3]=[C:2]([CH:7]=[CH:6][CH:5]=1)[N:10]([CH:11]1[CH2:15][CH2:14][CH2:13][CH2:12]1)[CH3:9]

Participants

Reactant 2

HCID 79271,3-Dibromobenzene

HCID 7020624N-methylcyclopentanamine

Product 1

HCID 66962129HCID 66962129, compound

Procedure

The title compound was prepared from 1,3-dibromobenzene and N-methylcyclopentanamine using a similar procedure to that described for D43. LCMS (A): m/z (M+H)+ 254/256, Cl2H16BrN requires 253/255 (acidic).

Sources & evidence

ORD record: ord-b2ed7d1fdff54d9b9df96dbd80a3b6eb
Source dataset: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08877742B2

Reaction notes

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