HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-bromo-6-hydroxy-1H-indenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromoindenone | HCID 9990649 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-bromo-6-hydroxy-1H-indenone | HCID 70317129 | — |
Reaction Steps
1 to 1.2 eq of the 2-bromo-1H-indenone prepared in Step 4 is dissolved in MeOH, and then K2CO3 (1 to 2 eq) is added thereto. The resulting mixture is stirred at room temperature for 2 to 7 h, to obtain the 2-bromo-6-hydroxy-1H-indenone of formula 8 in which acetyl group is removed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877747B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-65de89de0233422f994a3a1f0108cdff |
| Source note | uspto-grants-2014_11 |