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HRID33139

反应详情

EQUATION

反应方程式

HRID 33139 的结构方程式

REACTANTS

反应物

2
结构：Clc1ccc2nc(N3CCNCC3)sc2c1
HCID2746595

6-Chloro-2-(piperazin-1-yl)-1,3-benzothiazole

C11H12ClN3S

结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)O
HCID21100237

2-(1-Methylethoxy)-5-(methylsulfonyl)benzoic acid

C11H14O5S

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)N1CCN(c2nc3ccc(Cl)cc3s2)CC1
HCID11648903

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to example 1.1 b) from 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.2) and 6-chloro-2-piperazin-1-yl-benzothiazole. The crude material was purified by chromatography (SiO2, CH2Cl2/MeOH=95/5) to yield the title compound as a yellowish solid. MS (m/e): 552.3 (M+CH3COOH+)

WORKUP

后处理

  1. customThe crude material was purified by chromatography (SiO2, CH2Cl2/MeOH=95/5)