2-Methanesulfonylacetic acid → HCID 178504898, compound

Participants

Reaction Steps

The title compound, off-white solid (77 mg, 60%), MS (ISP) m/z=447.4 [(M+H)+], mp 201° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-4-yl-piperidin-1-yl)-ethyl]-cyclohexyl-amine dihydrochloride (intermediate A) (115 mg, 0.29 mmol) and 2-methanesulfonyl-acetic acid.

Provenance & Evidence