huagongshe.com
HRID33149

反应详情

EQUATION

反应方程式

HRID 33149 的结构方程式

REACTANTS

反应物

2
结构：CC(C)COc1ccc(S(C)(=O)=O)cc1C(=O)O
HCID23503110

未命名化合物

结构：CCS(=O)(=O)c1ccc2oc(N3CCNCC3)nc2c1.Cl
HCID68896068

未命名化合物

PRODUCTS

生成物

1
结构：CCS(=O)(=O)c1ccc2oc(N3CCN(C(=O)c4cc(S(C)(=O)=O)ccc4OCC(C)C)CC3)nc2c1
HCID58906319

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to example 1.1 b) from 2-isobutoxy-5-methanesulfonyl-benzoic acid (Example 2.4) and 5-ethanesulfonyl-2-piperazin-1-yl-benzoxazole hydrochloride. The crude material was purified by chromatography (SiO2, ethyl acetate) to yield the title compound as a colorless solid.

WORKUP

后处理

  1. customThe crude material was purified by chromatography (SiO2, ethyl acetate)