HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66823383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68077951 | HCID 68077951 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 66823383 | HCID 66823383 | — |
Reaction Steps
tert-Butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-{[methyl(propylsulfonyl)amino]methyl}phenyl)ethyl}carbamate (20.9 mg, 0.039 mmol) was treated with hydrochloric acid in isopropanol (5 M, 1 ml) at room temperature. The solvent was evaporated in vacuo. Water (1 ml) was added and the product was freeze-dried. Yield: 16 mg (0.034 mmol, 87%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877794B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-2833fdaa803d4db1aeece56a6936fcb1 |
| Source note | uspto-grants-2014_11 |