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HRID33188

反应详情

EQUATION

反应方程式

HRID 33188 的结构方程式

REACTANTS

反应物

3
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：CCN(CC)c1ccc(S(C)(=O)=O)cc1C(=O)O
HCID57445276

未命名化合物

结构：Cl.Clc1ccc2nc(N3CCNCC3)ccc2c1
HCID68896684

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)c1ccc(S(C)(=O)=O)cc1C(=O)N1CCN(c2ccc3cc(Cl)ccc3n2)CC1
HCID58906315

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Prepared in analogy to example 1.1 b) from 6-chloro-2-piperazin-1-yl-quinoline hydrochloride (Example 1.20b) and 2-diethylamino-5-methanesulfonyl-benzoic acid (Example 2.5) in acetonitrile. Chromatography (SiO2; ethyl acetate) yields the title compound as a colorless solid. MS (m/e): 501.4 (M+H+; 100%)