huagongshe.com
HRID33191

反应详情

EQUATION

反应方程式

HRID 33191 的结构方程式

REACTANTS

反应物

3
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：CS(=O)(=O)c1ccc(OCC2CC2)c(C(=O)O)c1
HCID21100228

2-(Cyclopropylmethoxy)-5-(methylsulfonyl)benzoic acid

C12H14O5S

结构：Cl.Clc1ccc2nc(N3CCNCC3)ccc2c1
HCID68896684

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1ccc(OCC2CC2)c(C(=O)N2CCN(c3ccc4cc(Cl)ccc4n3)CC2)c1
HCID58906304

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Prepared in analogy to example 1.1 b) from 6-chloro-2-piperazin-1-yl-quinoline hydrochloride (Example 1.20b) and 2-cyclopropylmethoxy-5-methanesulfonyl-benzoic acid (Example 2.6) in acetonitrile. Chromatography (SiO2; ethyl acetate) yields the title compound as a colorless solid. MS (m/e): 500.3 (M+H+; 100%)