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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 332595Generated: November 1, 2026

3-Amino-1-propanol → HCID 86003215, compound

https://huagongshe.com/reaction/332595

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Amino-1-propanolHCID 9086—
ReactantTriisopropylsilyl trifluoromethanesulfonateHCID 2724529—
SolventDichloromethaneHCID 6344—
ProductHCID 86003215HCID 86003215—

Reaction Steps

3-Hydroxylpropylamine (100 μL, 1.31 mmol) was dissolved in dichloromethane (4.4 mL), and triisopropylsilyl triflate (371 μL, 1.38 mmol) was added dropwise at room temperature. After stirring at room temperature for 15 minutes, the mixture was worked up according to a conventional method to give the title compound as a crude product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08877805B2
Source datasetuspto-grants-2014_11
ORD IDord-1f1e2e693332409b9da7f25293c22d3f
Source noteuspto-grants-2014_11