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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 332624Generated: October 31, 2026

HCID 77934570, compound → HCID 70869380, compound

https://huagongshe.com/reaction/332624

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 77934570HCID 77934570—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 70869380HCID 7086938057.7%

Reaction Conditions

Temperature50 °C

Reaction Steps

The compound (0.5 g, 1.4 mmol) obtained in step 3 was dissolved in ethanol (20 mL), palladium/carbon (0.1 g) was added, and the mixture was stirred at 50° C. for 20 hours under a hydrogen atmosphere (55 psi). The reaction mixture was filtered, and the solvent was evaporated under reduced pressure to give the title compound (0.3 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08877805B2
Source datasetuspto-grants-2014_11
ORD IDord-6015b547594349d9b02d899d458af548
Source noteuspto-grants-2014_11