HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 332624Generated: October 31, 2026
HCID 77934570, compound → HCID 70869380, compound
https://huagongshe.com/reaction/332624
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 77934570 | HCID 77934570 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70869380 | HCID 70869380 | 57.7% |
Reaction Steps
The compound (0.5 g, 1.4 mmol) obtained in step 3 was dissolved in ethanol (20 mL), palladium/carbon (0.1 g) was added, and the mixture was stirred at 50° C. for 20 hours under a hydrogen atmosphere (55 psi). The reaction mixture was filtered, and the solvent was evaporated under reduced pressure to give the title compound (0.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08877805B2 |
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| Source dataset | uspto-grants-2014_11 |
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| ORD ID | ord-6015b547594349d9b02d899d458af548 |
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| Source note | uspto-grants-2014_11 |
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