HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-(2-Bromo-4-cyanophenyl)-3-methylimidazolium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(2-Bromo-4-cyanophenyl)imidazole | HCID 68854444 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(2-Bromo-4-cyanophenyl)-3-methylimidazolium iodide | HCID 178480663 | — |
Reaction Steps
1-(2-Bromo-4-cyanophenyl)imidazole (5.4 g, 22 mmol, 1 eq) and methyl iodide (15.4 g, 109.0 mmol, 5 eq) are dissolved in tetrahydrofuran (50 ml) and stirred at room temperature for 16 hours. The precipitate formed is filtered off and washed with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877937B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-28d73abda1b7430bb1c5c08c68a27d33 |
| Source note | uspto-grants-2014_11 |