1,3-Propanediamine → HCID 66835428, compound

Participants

Reaction Conditions

Reaction Steps

4-Chloro-2-picoline (441 μl, 4 mmol) was mixed with 1,3-diaminopropane (1.67 ml, 20 mmol) and stirred in a closed vessel at 180° C. under microwave heating for one hour. The solvent was removed under reduced pressure, toluene was added to the residue and the mixture was evaporated to dryness under reduced pressure to yield 1.076 of a solid. MS (APCI) m/z=165.8 [M+H]+.

Provenance & Evidence