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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 333226생성일: 2026년 10월 26일

Trifluoroacetic acid → HCID 66819661, 화합물

https://huagongshe.com/reaction/333226

반응식

참여 물질

역할이름HCID투입량
반응물Trifluoroacetic acidHCID 6422—
반응물(6-{[(6-Oxo-5,6-dihydro-phenanthridin-2-ylcarbamoyl)-methyl]-amino}-hexyl)-carbamic acid tert-butyl esterHCID 66819636—
용매DichloromethaneHCID 6344—
생성물HCID 66819661HCID 6681966165%

반응 단계

(6-{[(6-oxo-5,6-dihydro-phenanthridin-2-ylcarbamoyl)-methyl]-amino}-hexyl)-carbamic acid tert-butyl ester was dissolved in dichloromethane (5 mL) and trifluoroacetic acid (1.5 mL) was added. The reaction mixture was stirred at room temperature overnight, evaporated, taken up with diethyl ether, filtered and the collected solid was dried under vacuum to afford 30 mg (65% yield) of the title compound as a light-yellow solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08877944B2
출처 데이터셋uspto-grants-2014_11
ORD IDord-3ce85afeef0641a89234fb1c9fc88e2d
출처 메모uspto-grants-2014_11