HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178466769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178466770 | HCID 178466770 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178466769 | HCID 178466769 | — |
Reaction Steps
2-(4-acetyl-phenylazo)-2-(3,3-dimethyl-3,4-dihydro-2H-isoquinoline-1-ylidene)-acetamide (Asinex Corp., Russia), thionyl chloride and DMF are mixed and stirred slowly. An excess of thionyl chloride is removed from the mixed solvent by reducing the pressure. The residue containing the reaction product is purified by column chromatography to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883504B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-185e46c3959f47cdae253a5af0d8ff7b |
| Source note | uspto-grants-2014_11 |